NEW extended VT HXMAS probe From -100 to 200 ℃ in narrow-bore magnet!
The wide temperature range HXMAS probe achieved -100 ～ 200℃ of sample temperature by a newly developed spinning module. This probe is available in a narrow-bore magnet due to newly designed thermal insulation and exhaust systems.
207Pb solid state NMR spectra for Pb(NO3)2 are shown in the following. The chemical shift of 207Pb signals indicate -100 ～ 200℃ of sample temperature.
* An additional option may be need to achieve 200℃ sample temperature.
* A heat-resistance zirconia sample tube is required above 150℃.
 A. Bielecki and D.P. Burum, J. Magn. Reson. A, 116, 215-220 (1995).
 T. Takahashi, et. al., Solid State Nuc. Magn. Reson., 15, 119-123 (1999).