To distinguish crystalline form of small molecule, powder X-ray diffraction and 13C CPMAS solid-state NMR are widely used. Here, we introduce a combined approach of 1H solid-state NMR at ultrafast MAS and electron diffraction using TEM to overcome the difficulty which powder X-ray and 13C CPMAS solid-state NMR have.
Oikawa, T., Okumura, M., Kimura, T. & Nishiyama, Acta Cryst. C73 (2017) 219–228.
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