AccuTOF™ GC series Materials and Chemistry Applications Notebook

  • Summary

Edition May 2020

JEOL Mass Spectrometer Material analysis solutions

This is a compendium of material science/engieering and chemistry related applications notes and JEOL News articles based on the data acquired on JEOL high resolution GC-TOFMS AccuTOF™ GC series (JMS-T100GC, JMS-T100GCV, JMS-T200GC).

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Table of Contents

Introduction   P1~

  • Development of an Integrated Analysis Method for the JMS-T200GC High Mass-Resolution GC-TOFMS by Electron Ionization and Soft Ionization Methods
    (Ubukata, M., Ueda, Y., JEOL news, 50, 83 – 89, 2019)
  • New Gas Chromatography / High Resolution Time-of-Flight Mass Spectrometer JMS-T200GC "AccuTOF™ GCx"
    (Ubukata, M., JEOL News, 50, 77 – 82, 2015)
  • Introduction of latest GC/HR-TOFMS system: JMS-T200GC AccuTOF™ GCx
    - High Mass Accuracy and Stability
  • Introduction of latest GC/HR-TOFMS system: JMS-T200GC AccuTOF™ GCx
    - High Mass Resolution
  • Introduction of latest GC/HR-TOFMS system: JMS-T200GC AccuTOF™ GCx
    - High Sensitivity Measurement
  • Comparison of performance between PI and FI by using GC-HRTOFMS
  • High-speed 50 Hz Data Acquisition Capability for Comprehensive 2-dimensional GC Measurements (MSTips No.226)
  • The Qualitative Analysis of an Antioxidant Additive Using the Full Capabilities of the EI/FI/FD Combination Ion Source (MSTips No.224)

Pyrolysis(Py)-GC/MS   P33~

  • Analyzing a Specific Component using Group Analysis of msFineAnalysis Ver. 2  (MSTips No.303) 
  • Integrated Analysis of an Acrylic Resin using msFineAnalysis v2 (MSTips No.300)
  • Comprehensive Analysis + Unknown Component Analysis of Vinyl Acetate Resins  Using Pyrolysis GC-MS (MSTips No.243)
  • Using Volcano Plots to Compare Vinyl Acetate Resin Samples Measured by Pyrolysis GC-MS (MSTips No.244)
  • Analysis of additives in plastic by thermal desorption (TD) GC-TOFMS 
    ~ accurate mass measurement and isotope pattern matching ~ (MS Tips No.138)
  • Analysis of acrylic resin by pyrolysis GC-TOFMS (MS Tips No.101)

Pyrolysis(Py)-GCxGC/MS   P45~

  • Identification and distribution analysis of additives in a molded NBR by PY/GCxGC/HRTOFMS (MSTips No.289) 
  • Ion Exchange Resin Analysis by using Pyrolysis-GCxGC-MS (MSTips No.274)
  • Ethylene Propylene Diene Monomer Rubber Analysis by using Pyrolysis-GCxGC-MS (MSTips No.273)
  • Natural Polymer Analysis by using Pyrolysis-GCxGC-MS
    -"Urushi" analysis with GCxGC/EI and GCxGC/PI- (MSTips No.245)

GC/MS   P53~

  • Integrated Analysis of Fatty Acid Methyl Esters using msFineAnalysis v2 (MSTips No.301)
  • Analysis of polydimethylsiloxanes by GC/TOFMS (MS Tips No.131)
  • GC/TOFMS analysis of high boiling point compounds ~cholesterol and Irganox 1010~ (MS Tips No.123) 
  • Analysis of photo polymerization initiator in UV light curing adhesives by GC/TOFMS  (MS Tips No.108)
  • Analysis of advanced materials by FD/FI using "AccuTOF™ GC" Part I
    ~ analysis of polymer building blocks with isocyanate and pilazole groups ~ (MS Tips No.089)
  • Analysis of advanced materials by FD/FI using "AccuTOF™ GC" Part II
    ~ analysis of multifunctional thiols, curing agents for functional polymers ~ (MS Tips No.090)
  • Detection of molecular ions of fluorine compounds by GC/FI-TOFMS (MS Tips No.088)
  • The Power of Exact Mass Measurement:
    An Example of Unknown Compound Identification (MS Tips No.040)

Direct Sample Introduction (Direct Probes, Field Desorption)   P71~

  • Analysis of polymer additives using DIP-EI and FD (MS Tipsv No.151)
  • Analysis of organogermanium compounds by field desorption (FD) ionization using JMS-T100GC "AccuTOF™ GC" (MS Tips No.121)
  • Analysis of ionic liquid by field desorption (FD) ionization using JMS-T100GC "AccuTOF™ GC"  (MS Tips No.113)
  • Analysis of block copolymer by field desorption (FD) using JMS-T100GC "AccuTOF™ GC" (MS Tips 110)
  • Analysis of advanced materials by FD/FI using "AccuTOF™ GC" Part III
    ~ analysis of organic borates, photoinitiators for polymerization ~ (MS Tips No.091)
  • Analysis of advanced materials by FD/FI using "AccuTOF™ GC" Part IV
    ~ analysis of NIR-photosensitive dyes ~ (MS Tips No.092)
  • Detection of molecular ions from OLED material using AccuTOF™ GC (MS Tips No.087)
  • Analysis of organic pigments using a direct exposure probe on JMS-T100GC "AccuTOF™ GC" (MS Tips No.085)
  • Analysis of organic EL material by JMS-T100GC "AccuTOF™ GC"
    ~ comparison of FD and DEI methods ~ (MS Tips No.078)

TG(Thermogravimetry)/MS, EGA (Evolved Gas Analysis)  P89~

  • Thermal decomposition analysis of antioxidant additive by TG-MS
    - Accurate mass measurement with TG-TOFMS system- (MSTips No.250)
  • Fluorocarbon polymers analysis by TG-MS
    - High m/z range measurement using TG-TOFMS system- (MSTips No.249) 
  • Evolved gas monitoring from PA66 by using PY-GC-HRTOFMS

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