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JMS-S3000 SpiralTOF™ series Polymers, Materials, & Chemistry Applications Notebook

Edition August 2023

This is a compendium of mass spectrometry imaging applications notes and JEOL News articles based on the data acquired on JEOL ultra-high mass-resolution MALDI-TOFMS JMS-S3000 SpiralTOF™ series.

Please see the PDF file for the additional information.
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Table of Contents

Introduction and Fundamentals P1〜

  • Development of JMS-S3000: MALDI-TOF/TOF Utilizing a Spiral Ion Trajectory (Takaya Satoh, JEOL News, 45, 34-37, 2010)

  • Development of peak extraction method from a high-resolution MALDI-TOF mass spectrum by machine learning focusing on peak shape, and an application to synthetic polymer analysis (MSTips No. 352)

  • The Relationship between Crystal Condition and Mass Resolving Power, Mass Accuracy (MSTips No. 206)

Synthetic Polymers

Spiral Mode / Linear Mode P15〜

  • Differential analysis of UV degradaed polyethylene terephthalate using JMS-S3000 "SpiralTOF™-plus2.0" and "msRepeatFinder" (MSTips No. 422)

  • Analysis of mPEG5K-Phosphate using JMS-S3000 "SpiralTOF™-plus 2.0" (MSTips No. 402)

  • Elemental Composition Determination of Polymer End Groups Using Accurate Mass (MSTips No. 357)

  • Structural analysis of anionic surfactants in MALDI negative ion mode using "SpiralTOF™- plus" (MSTips No. 333)

  • Analysis of degraded polymethyl methacrylate by UV irradiation using high-resolution MALDI-TOFMS and pyrolysis-GC-QMS (MSTips No. 324)

  • Analysis of degraded polystyrene by UV irradiation using high-resolution MALDI-TOFMS and pyrolysis-GC-QMS (MSTips No. 322)

  • "Fraction base" KMD plots for a high molecular weight poly(3-hydroxybutyrate-co-3- hydroxyvalerate) copolyester following its on-plate alkaline degradation and SpiralTOF™ analysis (MSTips No. 284)

  • "Fraction base" KMD plots for a high molecular weight poly(3-hydroxybutyrate) polyester following its on-plate alkaline degradation and SpiralTOF™ analysis" (MSTips No. 283)

  • "Remainders of KM" plot for polymers using msRepeatFinder: compositional mapping over a broad mass range (MSTips No. 269)

  • Analysis of low molecular weight polyethylene with solvent-free method using JMS-S3000 "SpiralTOF™" (MSTips No. 235)

  • Analysis of cyanoacrylate adhesive using the JMS-S3000 "SpiralTOF™" ― Application of Kendrick Mass Defect plot analysis ― (MSTips No. 220)

  • Measurement of a Dendritic MS Reference Standard

  • Analysis of EO-PO Random Copolymer by Using a Conventional HPLC and MALDI SpiralTOF™ MS (MSTips No. 203)

  • Analysis of high molecular weight polystyrene standards by using JMS-S3000 SpiralTOF™ with Linear TOF option (MSTips No. 199)

  • Measurement of Synthetic Polymers [1]: Polystyrene (MSTips No. 163)

  • Measurement of Synthetic Polymers [2]: Polymethyl Methacrylate (MSTips No. 164)

  • Measurement of Synthetic Polymers [3]: Polyethylene Glycol (MSTips No. 165)

  • Detailed Structural Characterization of Polymers by MALDI-TOFMS with a Spiral Ion Trajectory (Sato, H., JEOL News, 50, 46-52, 2015)

  • MALDI SpiralTOF™ high-resolution mass spectrometry and Kendrick mass defect analysis applied to the characterization of poly(ethylene-co-vinyl acetate) copolymers (Fouquet, T., Nakamura, S. & Sato, H., Rapid Commun. Mass Spectrom. 30, 973 – 981, 2016)

TOF-TOF (MS/MS) Mode P77〜

  • Structural analysis of polyethylene terephthalate combining an on-plate alkaline degradation method and tandem time-of-flight mass spectrometry (MSTips No. 311)

  • Visualizing fragmentation channels of polyethylene oxide with different end groups using the JMS-S3000 SpiralTOF™ with TOF–TOF option (MSTips No. 279)

  • "Remainders of KM" plot for polymers using msRepeatFinder: Intuitive display of High energy collision induced dissociation mass spectra acquired by SpiralTOF™/TOF (MSTips No. 270)

Polymer Additives P89〜

  • Structure analysis of a polymer additive using high-energy collision–induced dissociation mass spectra acquired by JMS-S3000 with TOF/TOF option (MSTips No. 254)

  • MALDI for Polymer Analysis: Synthetic Polymers and Additives (MSTips No. 205)

Organic Chemistry / Small Molecules P95〜

  • Measurement of boroxine cage using JMS-S3000 "SpiralTOF™ (MSTips No. 369)

  • Structural analysis of a small molecule using JMS-S3000 "SpiralTOF™-plus 2.0" ー MS/MS measurement of a photodegradation product of reserpine ー (MSTips No. 365)

  • Analysis of medicinal properties in a combination cold remedy by using JMS-S3000 "SpiralTOF™" (MSTips No. 241)

  • MALDI for Small Molecule Analysis: Triazine Pesticides

  • High-Energy CID MS-MS Analysis of Small Organic Molecules (MSTips No. 173)

  • MALDI for Small Molecule Analysis: A Complex Drug Mixture

  • Accurate mass measurement of small organic molecules using JMS-S3000 "SpiralTOF™" (MSTips No. 168)

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