JMS-S3000 SpiralTOF™ Series Polymers, Matrials, & Chemistry Applications Notebook

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Edition June 2020

JMS-S3000 SpiralTOF(TM) series Polymers, Materials, & Chemistry Applications Notebook

This is a compendium of applications notes, JEOL News articles, and scientific journal articles related to synthetic polymers, materials science/engineering, and chemistry based on the data acquired on JEOL ultra-high mass-resolution MALDI-TOFMS JMS-S3000 SpiralTOF™ series.

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Table of Contents

Introduction and Fundamentals P1~

  • Development of JMS-S3000: MALDI-TOF/TOF Utilizing a Spiral Ion Trajectory
    (Takaya Satoh, JEOL News, 45, 34-37, 2010)
  • The Relationship between Crystal Condition and Mass Resolving Power, Mass Accuracy  (MS Tips No.206) 

Synthetic Polymers

Spiral Mode / Linear Mode P11~

  • Detailed Structural Characterization of Polymers by MALDI-TOFMS with a Spiral Ion Trajectory
    (Sato, H., JEOL News, 50, 46-52, 2015)
  • MALDI SpiralTOF™ high-resolution mass spectrometry and Kendrick mass defect analysis applied to the characterization of poly(ethylene-co-vinyl acetate) copolymers
    (Fouquet, T., Nakamura, S. & Sato, H., Rapid Commun. Mass Spectrom. 30, 973 – 981, 2016)
  • "Fraction base" KMD plots for a high molecular weight poly(3-hydroxybutyrate-co-3-hydroxyvalerate) copolyester following its on-plate alkaline degradation and SpiralTOF™ analysis  (MSTips No.284)
  • "Fraction base" KMD plots for a high molecular weight poly(3-hydroxybutyrate) polyester following its on-plate alkaline degradation and SpiralTOF™ analysis (MSTips No.283)
  • "Remainders of KM" plot for polymers using msRepeatFinder: compositional mapping over a broad mass range  (MSTips No.269)
  • Analysis of low molecular weight polyethylene with solvent-free method using JMS-S3000 "SpiralTOF™" (MSTips No.235)
  • Analysis of cyanoacrylate adhesive using the JMS-S3000 "SpiralTOF™"
    ― Application of Kendrick Mass Defect plot analysis ― (MSTips No.220)
  • Measurement of a Dendritic MS Reference Standard
  • Analysis of EO-PO Random Copolymer by Using a Conventional HPLC and MALDI SpiralTOF™ MS (MS Tips No.203)
  • Analysis of high molecular weight polystyrene standards by using JMS-S3000 SpiralTOF™ with Linear TOF option  (MS Tips No.199)
  • Measurement of Synthetic Polymers [1]: Polystyrene (MS Tips No.163)
  • Measurement of Synthetic Polymers [2]: Polymethyl Methacrylate (MS Tips No.164)
  • Measurement of Synthetic Polymers [3]: Polyethylene Glycol (MS Tips No.165)

TOF-TOF (MS/MS) Mode P55~

  • Structural analysis of polyethylene terephthalate combining an on-plate alkaline degradation method and tandem time-of-flight mass spectrometry (MSTips No.311)
  • Visualizing fragmentation channels of polyethylene oxide with different end groups using the JMS-S3000 SpiralTOF™ with TOF–TOF option (MSTips No.279)
  • "Remainders of KM" plot for polymers using msRepeatFinder: Intuitive display of High energy collision induced dissociation mass spectra acquired by SpiralTOF™/TOF (MSTips No.270)
  • Synthetic Polymer Structure Analysis: Poly Propylene Glycol (PPG)  (MS Tips No.171)
  • Synthetic Polymer Structure Analysis: Polymethyl methacrylate  (MS Tips No.172)

Additives / Small Molecules P71~

  • Structure analysis of a polymer additive using high-energy collision–induced dissociation mass spectra acquired by JMS-S3000 with TOF/TOF option (MSTips No.254)
  • Analysis of medicinal properties in a combination cold remedy by using JMS-S3000 "SpiralTOF™" (MSTips No.241)
  • MALDI for Polymer Analysis: Synthetic Polymers and Additives (MS Tips No.205) 
  • MALDI for Small Molecule Analysis: Triazine Pesticides
  • High-Energy CID MS-MS Analysis of Small Organic Molecules (MS Tips No.173)
  • MALDI for Small Molecule Analysis: A Complex Drug Mixture
  • Accurate mass measurement of small organic molecules using JMS-S3000 "SpiralTOF™" (MS Tips No.168)

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